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The investigation of the interfacial phase transitions in fluid systems with short-range intermetallic interactions are of great interest. The phenomena were studied in two systems exhibiting a liquid-liquid miscibility gap: at the fluid/wall interface in fluid KxKCl1-x and at the fluid/vacuum interface of the Ga1 xBix alloys. To characterize the interfacial changes of the ultra thin films (composition, thickness and their evolution with time) the spectroscopic ellipsometry was performed over a wide spectral range. Whereas in the experiments on KxKCl1-x an existing ellipsometer could be used, a completely new UHV-apparatus including the in-situ phase modulation ellipsometer had to be developed for Ga1 xBix alloys. For the KxKCl1-x system new results on complete wetting at solid-liquid coexistence as well as in the homogenous liquid phase (prewetting) are presented. The spectra show the typical F center absorption which indicates that the film is a salt-rich phase. The thickness strongly increases approaching the monotectic from 30 to 440 nm, which is in agreement with the tetra point wetting scenario. For this interpretation a quantitative description of the excess Gibbs energy has been developed. For the Ga1 xBix system the results on complete wetting, surface freezing and oscillatory interfacial instabilities are presented. The high-precision spectra have been recorded approaching the liquid-liquid miscibility. These spectra have been modeled using a Ga-Bi effective medium approximation for the substrate covered by a film of liquid Bi. The measurements give evidence of tetra point wetting in the Ga-Bi system. First ellipsometric study of the surface freezing in Ga-Bi has been performed. Within the miscibility gap a very interesting effect of surface and bulk oscillatory instability was observed. The details of this process at present are not well understood, but a qualitative description is given.
molten salt --- surface phase transition --- spectroscopic ellipsometry --- Ga-Bi alloys
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Ellipsometry is rapidly emerging as a popular solution addressed to new materials science challenges and technological pitfalls hindering its effective application on modern problems. Amid the nowadays active development of materials of top notch, ellipsometry is also evolving rapidly both in the academic and industry sectors. The global industry strategies, introduce the latest scientific advances at manufacturing new, more accurate, and reliable ellipsometry systems to tackle emerging challenges. The book provides a comprehensive overview on the principles and technical capabilities of the modern ellipsometry highlighting its versatility in materials characterization.
Ellipsometry. --- Polarimetry --- Polarization (Light) --- Surfaces (Technology) --- Thin films --- Physical Sciences --- Engineering and Technology --- Optoelectronics --- Physics --- Optics and Lasers
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Ellipsometry is an experimental technique for determining the thickness and optical properties of thin films. It is ideally suited for films ranging in thickness from subnanometer to several microns. Spectroscopic measurements have greatly expanded the capabilities of this technique and introduced its use into all areas where thin films are found: semiconductor devices, flat panel and mobile displays, optical coating stacks, biological and medical coatings, protective layers, and more. While several scholarly books exist on the topic, this book provides a good introduction to the basic theory of the technique and its common applications. It follows in the footsteps of two previous books written by one of the authors with important updates to emphasize modern instrumentation and applications. The target audience is not the ellipsometry scholar, but process engineers and students of materials science who are experts in their own fields and wish to use ellipsometry to measure thin film properties without becoming an expert in ellipsometry itself.
Ellipsometry. --- Thin films --- Spectrum analysis --- Analysis, Spectrum --- Spectra --- Spectrochemical analysis --- Spectrochemistry --- Spectrometry --- Spectroscopy --- Chemistry, Analytic --- Interferometry --- Optics --- Radiation --- Wave-motion, Theory of --- Absorption spectra --- Light --- Spectroscope --- Films, Thin --- Solid film --- Solid state electronics --- Solids --- Surfaces (Technology) --- Coatings --- Thick films --- Polarimetry --- Polarization (Light) --- Measurement. --- Qualitative --- Cauchy equation --- dispersion equations --- ellipsometry --- optical constants --- polarized light --- refractive index --- thin film thickness --- Analytical chemistry
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The book is devoted to the design, application and characterization of thin films and structures, with special emphasis on optical applications. It comprises ten papers—five featured and five regular—authored by scientists all over the world. Diverse materials are studied and their possible applications are demonstrated and discussed—transparent conductive coatings and structures from ZnO doped with Al and Ga and Ti-doped SnO2, polymers and nanosized zeolite thin films for optical sensing, TiO2 with linear and nonlinear optical properties, organic diamagnetic materials, broadband optical coatings, CrWN glass molding coatings, and silicon on insulator waveguides.
faraday rotation --- thin films --- magneto-optics --- organic material --- tolane derivatives --- optical coatings --- monitoring --- deposition --- titanium dioxide --- optical constants --- two-photon absorption --- nonlinear refraction --- scattering --- laser-induced deflection --- absorption measurement --- CrWN coatings --- microstructure evolution --- spinodal decomposition --- thermal stability --- hardness --- plasma enhanced magnetron sputtering --- sidewall roughness --- optical scattering loss --- silicon-on-insulator waveguide --- multilayer --- ZnO --- Ag --- TCO --- transmittance --- structure --- resistance --- SnO2 --- Ti-doped --- annealing temperature --- electrical resistivity --- optical sensors --- optical materials --- zeolites --- ellipsometry --- single wavelength ellipsometry --- spectroscopic ellipsometry --- poly(vinyl alcohol) copolymers --- humidity sensing --- Al-doped ZnO --- ALD technique --- transparent conductive layers --- LC display --- flexible PDLC devices --- transparent conductive coatings --- optical sensing --- broadband design --- linear and non-linear optical properties --- organic diamagnetic materials
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This 2001 book provides a detailed introduction to the principles of Doppler and polarimetric radar, focusing in particular on their use in the analysis of weather systems. The design features and operation of practical radar systems are highlighted throughout the book in order to illustrate important theoretical foundations. The authors begin by discussing background topics such as electromagnetic scattering, polarization, and wave propagation. They then deal in detail with the engineering aspects of pulsed Doppler polarimetric radar, including the relevant signal theory, spectral estimation techniques, and noise considerations. They close by examining a range of key applications in meteorology and remote sensing. The book will be of great use to graduate students of electrical engineering and atmospheric science as well as to practitioners involved in the applications of polarimetric radar systems.
Radar meteorology. --- Doppler radar. --- Polariscope. --- Polarimeter --- Optical instruments --- Doppler effect --- Radar --- Meteorology --- Radio waves --- Polarimetry. --- Polarization --- Measurement. --- Optical measurements --- Polarization (Light) --- Ellipsometry --- Hertzian waves --- Electric waves --- Electromagnetic waves --- Radio frequency --- Radio meteorology --- Signal theory (Telecommunication)
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This handbook has been prepared as a working reference for the safety officer, the environmental engineer, and the consultant. For the safety officer, this handbook provides detailed guidelines and instructions in preparing Right-to-Know Reporting Audits, establishing programs and training employees on hazard awareness, and developing and implementing emergency response programs in the workplace and at off-site operations.For the environmental engineer, this handbook provides extensive technical data on toxic chemical properties and detailed instructional aid on how to properly
Ellipsometry --- Polarimetry --- Polarization (Light) --- Surfaces (Technology) --- Thin films --- Engineering --- Electronics --- Ellipsometry. --- Chemical spills --- Hazardous substances --- 614.75 --- Dangerous chemicals --- Dangerous goods --- Dangerous materials --- Dangerous substances --- Hazardous chemicals --- Hazardous goods --- Hazardous materials --- Hazmats --- Chemicals --- Materials --- Spills, Chemical --- Pollution --- Reporting&delete& --- Handbooks, manuals, etc --- Accidents&delete& --- Safety measures&delete& --- Accidents --- 614.75 Precautions with, and handling of, noxious and dangerous substances --- Precautions with, and handling of, noxious and dangerous substances --- General and Others --- Reporting --- Safety measures
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This book contains the articles collected for the Special Issue entitled "Micro-nano Surface Functionalization of Materials and Thin Films for Optical Applications" in the journal Coatings (ISSN 2079-6412). These selected articles provide a meaningful overview of recent advances and concepts beyond the state-of-the-art regarding surface functionalization of materials and deposition of thin films to be used in optical applications. The aim was to cover all relevant aspects of the topic (simulation, design, fabrication, characterization and applications) with a special emphasis on non-conventional methods for surface modification of materials, combinations of mature fabrication routes with emerging technologies (i.e., additive manufacturing) and large-area fabrication concepts to pave the way to an industrial utilization of the developed materials. This overview comprises the recent work of reputed scientists from Germany, Austria, Spain and India on: - New developments on the scale-up deposition of transparent conductive materials by magnetron sputtering,- Design of hierarchical surface structures at different scale lengths for nanoimprinting of optical nano- and micro-structures, - Non-conventional preparation of rutile-type TiO2 films at room temperature for optical applications on heat-sensitive substrates, - Design of spectrally selective solar absorber coatings based on computational simulation and ellipsometry measurements.
reactive magnetron sputtering --- transparent conductive oxide --- electronic transport --- doping efficiency --- tin dioxide --- Nanoimprint lithography --- UV-NIL --- reversal NIL --- liquid transfer imprint lithography --- hierarchical structures --- optical micro- and nanostructures --- ITO thin films --- magnetron sputtering --- low temperature deposition --- oxygen flow --- microstructure --- optoelectronic properties --- transparent heaters --- titanium oxide films --- filtered cathodic vacuum arc --- rutile --- optical coatings --- spectrally selective absorber --- multilayer stack --- spectroscopic ellipsometry --- optical constants --- simulation
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This book is composed of 6 papers. The first paper reports a novel technique for the selective emitter formation by controlling the surface morphology of Si wafers. Selective emitter (SE) technology has attracted renewed attention in the Si solar cell industry to achieve an improved conversion efficiency of passivated-emitter rear-contact (PERC) cells. In the second paper, the temperature dependence of the parameters was compared through the PERC of the industrial-scale solar cells. As a result of their analysis, PERC cells showed different temperature dependence for the fill factor loss as temperatures rose. The third paper reports the effects of carrier selective front contact layer and defect state of hydrogenated amorphous silicon passivation layer/n-type crystalline silicon interface. The results demonstrated the effects of band offset determined by band bending at the interface of the passivation layer and carrier selective front contact layer. In addition, the nc-SiOx: H CSFC layer not only reduces parasitic absorption loss but also has a tunneling effect and field-effect passivation. The fourth paper reports excimer laser annealing of hydrogenated amorphous silicon film for TOPCon solar cell application. This paper analyzes the crystallization of a-Si:H via excimer laser annealing (ELA) and compared this process with conventional thermal annealing. The fifth paper reports the contact mechanism between Ag–Al and Si and the change in contact resistance (Rc) by varying the firing profile. Rc was measured by varying the belt speed and peak temperature of the fast-firing furnace. The sixth paper reports a silicon tandem heterojunction solar cell based on a ZnO/Cu2O subcell and a c-Si bottom subcell using electro-optical numerical modeling. The buffer layer affinity and mobility together with a low conduction band offset for the heterojunction are discussed, as well as spectral properties of the device model.
fill factor loss analysis --- double-diode model --- PERC --- temperature dependence --- recombination current density --- parasitic resistance --- carrier selective contact --- rear emitter heterojunction --- passivation --- crystallinity --- thermal annealing --- excimer laser annealing --- amorphous hydrogenated silicon film --- metallization --- contact formation --- Ag/Al paste --- p+ emitter --- N-type bifacial solar cells --- silicon tandem heterojunction solar cell --- N-doped Cu2O absorber layer --- Al:ZnO (AZO) --- numerical electro-optical modeling --- scanning electron microscopy (SEM) --- atomic force microscopy (AFM) --- X-ray diffraction (XRD) --- spectroscopic ellipsometry (SE) --- Fourier-transform infrared (FTIR) spectroscopy --- degradation degree --- failure rate --- selective emitter --- surface morphology --- doping process --- solar cell
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A compilation of 12 original research articles and a review on the development of instrumental and immunoanalytical methods for mycotoxins; on the enhancement of sample preparation and selection to improve method applicability; and on practical applications of analytical methods in laboratory fungal cultures, cereal and feed samples, surface water (as a novel matrix of mycotoxins as emerging surface water contaminants), and during mycotoxin decontamination by bacteria. Target analyte mycotoxins include aflatoxins, deoxynivalenol, diacetoxyscirpenol, fumonisins, fusarenone-X, HT-2 toxins, nivalenol, ochratoxins, sterigmatocystin, T-2 toxin, and zearalenone.
aflatoxins --- laboratory culture --- extraction --- HPLC --- recovery --- detection limits --- frequency mixing technology --- immunofiltration --- magnetic beads --- mycotoxin --- type B trichothecenes --- modified mycotoxins --- isomer separation --- method validation --- ochratoxin A --- fluorescence --- G-quadruplex --- biosensor --- computation --- simulation --- mycotoxins --- feed --- modified QuEChERS --- LC-MS/MS --- zearalenone --- immunochromatographic assay --- semi-quantification --- quantification --- aflatoxin B1 --- sterigmatocystin --- lactobacilli --- mycotoxin binding --- detoxification --- lactic acid bacteria --- colorimetric detection --- rapid tests --- ELISA --- lateral flow assays --- microfluidics --- nano-materials --- food safety --- commercialization --- immunosensor --- optical waveguide lightmode spectroscopy --- label-free detection --- planar waveguide sensor --- polarisation interferometer --- limit of detection --- competitive immunoassay --- fluorescence detection --- high-performance liquid chromatography --- total internal reflection ellipsometry --- aflatoxin --- chicken feed --- representative sampling --- improved aflatoxin test procedure --- validation --- n/a
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Despite its limitation in terms of surface covered area, the PLD technique still gathers interest among researchers by offering endless possibilities for tuning thin film composition and enhancing their properties of interest due to: (i) the easiness of a stoichiometric transfer even for very complex target materials, (ii) high adherence of the deposited structures to the substrate, (iii) controlled degree of phase, crystallinity, and thickness of deposited coatings, (iv) versatility of the experimental set-up which allows for simultaneous ablation of multiple targets resulting in combinatorial maps or consecutive ablation of multiple targets producing multi-layered structures, and (v) adjustment of the number of laser pulses, resulting in either a spread of nanoparticles, islands of materials or a complete covering of a surface. Moreover, a variation of PLD, known as Matrix Assisted Pulsed Laser Evaporation, allows for deposition of organic materials, ranging from polymers to proteins and even living cells, otherwise difficult to transfer unaltered in the form of thin films by other techniques. Furthermore, the use of laser light as transfer agent ensures purity of films and pulse-to-pulse deposition allows for an unprecedented control of film thickness at the nm level. This Special Issue is a collection of state-of-the art research papers and reviews in which the topics of interest are devoted to thin film synthesis by PLD and MAPLE, for numerous research and industry field applications, such as bio-active coatings for medical implants and hard, protective coatings for cutting and drilling tools withstanding high friction and elevated temperatures, sensors, solar cells, lithography, magnetic devices, energy-storage and conversion devices, controlled drug delivery and in situ microstructuring for boosting of surface properties.
thin films --- matrix-assisted pulsed laser evaporation --- shellac --- enteric coatings --- PLD --- ITO --- nanoimprint lithography --- coatings --- nanostructure --- iron oxide --- pulsed laser deposition --- aluminum nitride --- nanoindentation testing --- TEM imaging --- FTIR spectroscopy --- ellipsometry --- complex refractive index --- composite coatings --- MAPLE --- Lactoferrin --- macrophage interactions --- animal-origin calcium phosphate coatings --- natural hydroxyapatite --- doping --- high adherence --- pulsed laser deposition technique --- biomimetic applications --- target preparation --- room temperature ferromagnetism --- dilute magnetic semiconductor --- Indium oxide --- (InFe)2O3 --- PLD films --- energy storage --- thin-film electrodes --- thin-film solid electrolyte --- lithium microbatteries --- calcium phosphate-based coatings --- synthetic and natural hydroxyapatite --- in vivo testing --- biomedical applications --- n/a
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