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In der vorliegenden Arbeit wurde ein elektrochemisches Raster-Sonden-Mikroskop dazu benutzt, gezielt Nanostrukturen herzustellen und zu charakterisieren. Das elektrochemische Umfeld bietet gegenüber den sonst angewandten Techniken den Vorteil, dass die Über- und Untersättigung an den beiden Arbeitselektroden frei eingestellt werden kann. Diese Methode erlaubt es lokal Nanostrukturen definierter Größe herzustellen. Mittels einer selbst aufgebauten UHV-Apparatur konnten Präparationstechniken zur reproduzierbaren Herstellung von geometrisch hoch definierten STM-Spitzen für nahezu jedes Metall entwickelt werden. Derart qualitativ hochwertige STM-Spitzen ermöglichten erstmals einen Strommessbereich von 10-6 bis10-12 Ampere abzudecken. Die entwickelten Instrumente konnten zur Untersuchung der Systeme Co bzw. Ni auf Au(111)-Substraten eingesetzt werden. Das Verfahren zur Erzeugung magnetischer Nanostrukturen wurde optimiert und erste spektroskopische Messungen an der Fest-/ Flüssiggrenzfläche konnten durchgeführt werden.
Scanning tunneling microscopy. --- Scanning probe microscopy.
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The atomic force microscope (AFM) has become one of the leading nanoscale measurement techniques for materials science since its creation in the 1980's, but has been gaining popularity in a seemingly unrelated field of science: biology. The AFM naturally lends itself to investigating the topological surfaces of biological objects, from whole cells to protein particulates, and can also be used to determine physical properties such as Young's modulus, stiffness, molecular bond strength, surface friction, and many more. One of the most important reasons for the rise of biological AFM is that you can measure materials within a physiologically relevant environment (i.e. liquids). This book is a collection of works beginning with an introduction to the AFM along with techniques and methods of sample preparation. Then the book displays current research covering subjects ranging from nano-particulates, proteins, DNA, viruses, cellular structures, and the characterization of living cells.
Atomic force microscopy. --- Pathology. --- Disease (Pathology) --- Medical sciences --- Diseases --- Medicine --- Medicine, Preventive --- AFM (Microscopy) --- Scanning probe microscopy --- Medical microbiology & virology
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Atomic force microscopy is a surface analytical technique used in air, liquids or a vacuum to generate very high-resolution topographic images of a surface, down to atomic resolution. This book is not only for students but also for professional engineers who are working in the industry as well as specialists. This book aims to provide the reader with a comprehensive overview of the new trends, research results and development of atomic force microscopy. The chapters for this book have been written by respected and well-known researchers and specialists from different countries. We hope that after studying this book, you will have objective knowledge about the possible uses of atomic force microscopy in many scientific aspects of our civilisation.
Analytical chemistry. --- Atomic force microscopy. --- AFM (Microscopy) --- Scanning probe microscopy --- Analysis, Chemical --- Analytic chemistry --- Chemical analysis --- Chemistry, Analytic --- Chemistry --- Physical Sciences --- Engineering and Technology --- Analytical Chemistry --- Instrumental Chemistry
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This book is a collection of research papers that describe some of the latest research on lithium niobate, which is an important material with many technological applications. The papers fall into three sections, which respectively consider the relationship between photorefractive properties and the defect structure of lithium niobate, powder preparation using a wet chemistry method and high-energy ball-milling technique, and finally the investigation of the domain structures, stability and conduction, and applications in waveguide devices.
lithium niobate --- optical storage materials --- photorefractive materials --- high-energy ball-milling --- nanocrystals --- mechanochemical reaction --- chemical composition --- powders --- microparticles --- photonic electric-field sensor --- titanium diffused optical channel waveguide --- lithium–niobate electro-optic effect --- Y-fed balanced-bridge Mach-Zehnder interferometer (YBB-MZI) --- electro-optic modulator --- lithium niobate thin film --- proton exchange --- Mach-Zehnder --- integrated optics devices --- doping magnesium --- Bridgman method --- high homogeneity --- thermal stability --- nano-domain --- LNOI --- pre-heat treatment --- divalent --- trivalent --- tetravalent --- pentavalent and hexavalent doping --- computer modelling --- photorefractive properties --- defect structure --- conducting domain walls --- ferroelectric films --- lithium niobate-on-insulator --- scanning probe microscopy --- non-volatile memory
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